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1 article(s) from Křížek, Tomáš

Synthesis and supramolecular properties of regioisomers of mononaphthylallyl derivatives of γ-cyclodextrin

Markéta Bláhová,
Sergey K. Filippov,
Lubomír Kováčik,
Jiří Horský,
Simona Hybelbauerová,
Zdenka Syrová,
Tomáš Křížek and
Jindřich Jindřich

Beilstein J. Org. Chem. 2017, 13, 2509–2520, doi:10.3762/bjoc.13.248

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Scheme 1: Preparation of 2^I-O-, 3^I-O- and 6^I-O-naphthylallyl derivatives of γ-CD by cross-metathesis.

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Scheme 2: Preparation of 2-O-, 3-O- and 6-O-NA derivatives of γ-CD by direct alkylation (see Table 1 for the yields ...

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Figure 1: Volume-weighted distribution functions for water solutions of 2-O- (2a), 3-O- (2b), and 6-O- (2c) N...

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Figure 2: Distribution functions for 2-O- (2a), 3-O- (2b), and 6-O- (2c) NA-γ-CD regioisomers in 50% MeOH (v/...

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Figure 3: Volume-weighted distribution functions for the 3-O- (2b) and 6-O- (2c) NA-γ-CD regioisomer at diffe...

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Figure 4: Effect of increasing concentration and sonication on the morphology of the 3-O-derivative 2b. A to ...

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Figure 5: Effect of increasing concentration and sonication on the morphology of the 2-O-derivative 2a. A: 2 ...

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Figure 6: Effect of increasing concentration and sonication on the morphology of the 6-O-derivative 2c. A: 0....

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Figure 7: Heat change for injection per mole of NA-γ-CD added as a function of the total concentration of NA-...

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Figure 8: ¹H NMR spectra of 2-O-derivative 2a in D₂O at concentrations of 100, 10, and 1 mM.

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Figure 9: ¹H NMR spectra of 3-O-derivative 2b in D₂O at concentrations of 100, 10, and 1 mM.

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Figure 10: Putative objects and interactions in naphthylallyl-γ-CD solution, depicted schematically for 6^I-O-n...

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Published 27 Nov 2017

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